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HIGHLIGHTS - Anionic Polymerization: High Vacuum Techniques - High vacuum technique is a very important part for the realization of the synthetic strategy leading to well-defined macromolecules by anionic polymerization. In this Highlight the glass apparatuses and reactors, used for purification of reagents and reactions, as well as the high vacuum methodology are described. A few examples concerning the synthesis of model polymers with complex architectures are also presented/
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